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MEC5017 MODERN TECHNIQUES OF MATERIALS CHARACTERIZATION L T P C 3 0 0 3 CHARACTERIZATION Materials characterization - definition; importance and application with case studies, Ultra high vacuum, surface science DIFFRACTION METHODS Principles and general methods of compositional, structural and defect characterization, techniques of X-ray, electron and neutron diffraction, EDAX, THERMAL ANALYSIS Thermal methods - DTA, TGA, DSC, TMA and DMA. MICROSCOPIC ANALYSIS Microscop
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  MEC5017 MODERN TECHNIQUES OF MATERIALS CHARACTERIZATION L T P C 3 0 0 3 CHARACTERIZATION Materials characterization - definition; importance and application with case studies, Ultra high vacuum, surface science DIFFRACTION METHODS Principles and general methods of compositional, structural and defect characterization, techniques of X-ray, electron and neutron diffraction, EDAX, THERMAL ANALYSIS Thermal methods - DTA, TGA, DSC, TMA and DMA. MICROSCOPIC ANALYSIS Microscopy - optical, Electron microscopy  –   Transmission Electron Microscope (TEM), Scanning Electron Microscope (SEM), basic principle and instrumentation configuration - Atomic force microscope (AFM) including contact-mode, tapping-mode and lateral-force AFM, scanning tunneling microscope (STM), electron microprobe analysis. SPECTROSCOPIC ANALYSIS Optical spectroscopy - UV, visible, IR and Raman spectroscopy, ESCA and Auger spectroscopy - Fourier-transform infrared spectroscopy (FTIR) and Raman spectroscopy, including basic principle, instrumentation configuration, data interpretation and analysis. TEXTBOOKS 1.   Surface Analysis - The Principal Techniques , by John C. Vickerman, John Wiley &Sons; 1st edition, (1997), ISBN: 0471972924 2.   Organic Structural Spectroscopy by Joseph B. Lambert, Herbert F. Shurvell, David A Lightner, Robert Graham Cooks, Prentice Hall; 1st edition, (1997), ISBN: 0132586908 REFERENCES: 1.   Online AFM textbook, “Fundamentals of the scanning probe microscopy” by V. L.Mironov 2.   Surface Analysis Methods in Materials Science by D.J. O'Connor, Brett A. Sexton, 3.   Roger S. C. Smart, Springer; 2 edition, (2003), ISBN: 3540413308 4.   Organic Spectroscopy, by Lal Dhar Singh Yadav, Springer; 1 edition, (2005), ISBN:1402025742 5.   Surface and Thin Film Analysis: A Compendium of Principles, Instrumentation, and Applications by Henning Bubert , Holger Jenett, Wiley-VCH, (2002), ISBN: 3527304584 6.   “Scanning Probe Microscopy: The Lab on a Tip” by Ernst Meyer, Hans J. Hug, Roland Bennewitz, Springer, (2003), ISBN: 3540431802. 7.   Handbook of Surface and Interface Analysis, by John C. Riviere, CRC; 1 edition, (1998), ISBN: 0824700805 8.   Structure Determination of Organic Compounds : Tables of Spectral Data ,by E. Pretsch, P. Bühlmann, C. Affolter, Springer; 3 edition, (2004), ISBN: 3540678158 9.   Practical Guide to Surface Science and Spectroscopy by Yip-Wah Chung, Academic Press, (2001), ISBN: 0121746100.  MEC5021 COMPOSITE MATERIALS TECHNOLOGY L T P C 3 0 0 3 [Common for M.Tech (CAD/CAM) and M.Tech (Energy Engineering)] INTRODUCTION  Limitations of conventional materials - definition of composite materials - types and characteristics - applications. MATERIALS Fibbers - Materials - Fibber reinforced plastics - thermoset polymers - Coupling agents, fillers and additives - Metal Matrix and Ceramic composites. MANUFACTURING Fundamentals - bag moulding - compression moulding pultrusion-filament winding - other manufacturing process - quality inspection and non-destructive testing. MECHANICS AND PERFORMANCE Introduction to micro-mechanics-unidirectional lamina - laminates - interlaminar stresses - static mechanical properties - fatigue properties - impact properties - environmental effects - fracture mechanics and toughening mechanisms, damage prediction, failure modes. DESIGN Failure predictions - design considerations - joint design - codes - design examples. Optimization of laminated Composites - Application of FEM for design and analysis of laminated composites. Text Books: 1. Ronald Gibson, Principles of Composite Material Mechanics , Tata McGraw Hill, 1994. 2. Micael hyer, Stress Analysis of Fiber - Reinforced Composite Materials , Tata McGrawHill, 1998. References: 1. P.K.Mallicak, Fiber-reinforced composites , Monal Deklar Inc., New York, 1988. 2. B.D. Agarwal and L.J.Broutman, Analysis and Performance of Fiber Composites , John Wiley and Sons, New York, 1980. 3. F.L.Matthews & R.D.Rawlings, Composite Materials, Engineering and Sciences , Chapman & hall, London, 1994.
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